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Sodium Alginate Specifications of Commercial Pure & BP Ph Eur USP NF IP Analytical Reagent FCC Food Grade Manufacturers & Exporters

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Sodium Alginate CAS Number 9005-38-3

Sodium Alginate USP NF Grade Specifications:
(C6H7NaO6)n
Alginic acid, sodium salt;
Sodium alginate CAS 9005-38-3

DEFINITION
Sodium Alginate is the purified carbohydrate product extracted from brown seaweeds by the use of dilute alkali. It consists chiefly of the sodium salt of Alginic Acid, a polyuronic acid composed of β-d-mannuronic acid residues linked so that the carboxyl group of each unit is free while the aldehyde group is shielded by a glycosidic linkage. It contains NLT 90.8% and NMT 106.0% of sodium alginate of average equivalent weight 222.00, calculated on the dried basis.

IDENTIFICATION
A.
Sample solution: A solution (1 in 100)
Analysis: To 5 mL of Sample solution add 1 mL of calcium chloride.
Acceptance criteria: A voluminous, gelatinous precipitate is formed immediately.
B.
Sample solution: A solution (1 in 100)
Analysis: To 10 mL of Sample solution add 1 mL of 4 N sulfuric acid.
Acceptance criteria: A heavy, gelatinous precipitate is formed.

ASSAY
Alginates by specified procedure.
Sample: 250 mg
Analysis: Each mL of 0.2500 N sodium hydroxide consumed is equivalent to 27.75 mg of sodium alginate.
Acceptance criteria: 90.8% to 106.0% on the dried basis

Arsenic: NMT 1.5 ppm
Lead: To pass the test. --- NMT 10 ppm)
Microbial Enumeration Tests and Tests for Specified Microorganisms: The total bacterial count does not exceed 200 cfu/g, and the tests for Salmonella species and Escherichia coli are negative.
Loss on Drying: Dry a sample at 105C for 4 h: it loses NMT 15.0% of its weight.
Articles for Botanical Origin: Proceed as directed in Methods of Analysis, carefully igniting 3 g in a tared platinum dish, until the residue is thoroughly carbonized (5 min), and then igniting in a muffle furnace at a temperature of 800±25C until the carbon is completely burned off (approximately 75 min).
Acceptance criteria: 18.0% to 27.0% of ash on the dried basis
Packaging and Storage: Preserve in tight containers.

Specifications of Sodium Alginate BP Ph Eur Grade
Ph Eur
Action and use: Excipient.

DEFINITION
Sodium alginate consists mainly of the sodium salt of alginic acid, which is a mixture of polyuronic acids [C6H8O6)n] composed of residues of D-mannuronic acid and L-guluronic acid. Sodium alginate is obtained mainly from algae belonging to the Phaeophyceae.

CHARACTERS
Appearance: White or pale yellowish-brown powder.
Solubility: Slowly soluble in water forming a viscous, colloidal solution, practically insoluble in ethanol (96 per cent).

IDENTIFICATION
A. Dissolve 0.2 g with shaking in 20 ml of water. To 5 ml of this solution add 1 ml of calcium chloride solution. A voluminous gelatinous mass is formed.
B. To 10 ml of the solution prepared in identification test A add 1 ml of dilute sulphuric acid. A gelatinous mass is formed.
C. To 5 mg add 5 ml of water, 1 ml of a freshly prepared 10 g/l solution of 1,3-dihydroxynaphthalene in ethanol (96 per cent) and 5 ml of hydrochloric acid. Boil for 3 min, cool, add 5 ml of water, and shake with 15 ml of di-isopropyl ether. Carry out a blank test. The upper layer obtained with the substance to be examined exhibits a deeper bluish-red colour than that obtained with the blank.
D. It complies with the test for sulphated ash. The residue obtained, dissolved in 2 ml of water, gives reaction (a) of sodium.

TESTS
Solution S: Dissolve 0.10 g in water, with constant stirring, dilute to 30 ml with the same solvent and allow to stand for 1 h.
Appearance of solution: The solution is not more opalescent than reference and not more intensely coloured than intensity 6 of the range of reference solutions of the most appropriate colour.
Dilute 1 ml of solution S to 10 ml with water R.
Chlorides: Maximum 1.0 per cent.
Calcium: Maximum 1.50 per cent.
Heavy metals: Maximum 20 ppm.
Loss on drying: Maximum 15.0 per cent, determined on 0.1000 g by drying in an oven at 105C for 4 h.
Sulphated ash: 30.0 per cent to 36.0 per cent (dried substance), determined on 0.1000 g.
Microbial contamination: Total viable aerobic count not more than 103 micro-organisms per gram, determined by plate-count. It complies with the tests for Escherichia coli and Salmonella.


Specifications of Sodium Alginate FCC Food Grade
Algin
(C6H7O6Na)n Equiv wt, calculated 198.11
Equiv weight, actual (avg.) 222.00
INS: 401 CAS: 9005-38-3

DESCRIPTION
Sodium Alginate
occurs as a white to yellow-brown, fibrous or granular powder. It is the sodium salt of alginic acid. It dissolves in water to form a viscous, colloidal solution. It is insoluble in alcohol and in hydroalcoholic solutions in which the alcohol content is greater than about 30% by weight. It is insoluble in chloroform, in ether, and in acids having a pH lower than about 3.
Function: Stabilizer; thickener; emulsifier; gelling agent.

REQUIREMENTS
Identification: -
A. Add 1 mL of calcium chloride to 5 mL of a 1:100 aqueous solution. A voluminous, gelatinous precipitate forms.
B. Add 1 mL of 2 N sulfuric acid to 10 mL of a 1:100 aqueous solution. A heavy, gelatinous precipitate forms.
C. Place about 5 mg of sample into a test tube, add 5 mL of water, 1 mL of a freshly prepared 1:100 naphtholresorcinol:ethanol solution, and 5 mL of hydrochloric acid. Heat the mixture to boiling, boil gently for about 3 min, and then cool to about 15C. Transfer the contents of the test tube to a 30-mL separator with the aid of 5 mL of water, and extract with 15 mL of isopropyl ether. Perform a blank determination and make any necessary correction. The isopropyl ether extract from the sample exhibits a deeper purple hue than that from the blank.
Assay: A sample yields not less than 18.0% and not more than 21.0% of carbon dioxide (CO2), corresponding to between 90.8% and 106.0% of Sodium Alginate (equiv wt 222.00).
Arsenic: Not more than 3 mg/kg.
Lead: Not more than 5 mg/kg.
Loss on Drying: Not more than 15.0%.

SDS MSDS of Sodium Alginate BP Ph Eur EP JP USP NF IP ACS Analytical Reagent FCC Food grade Manufacturers

Crystal Clear Products and the group companies are manufacturing chemicals since several decades. We have automatic vacuum operated titanium evaporators and SS316 equipments to produce top grade of chemical products. We have toll manufacturers and representatives in China, UAE, Europe, Canada & USA and agents & customers in all countries like USA, Canada, Europe, UAE, South Africa, Tanzania, Kenya, Egypt, Nigeria, Uganda, Turkey, Mexico, Brazil, Chile, Argentina, Bangkok Thailand, Kaula Lumpur Malaysia, Dubai UAE etc. & sales representative in Chicago, Houston New York & Los Angeles, USA. Associated units are FDA-GMP certified, Halal and/or Kosher certified, REACH registered, ISO-9001, ISO-22000 HACCP certified, Crisil Rated.

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Crystal Clear Products
Plot No-C1-1031-9, GIDC Estate, Panoli, Ankleshwar, Gujarat - 393002. India
Telephone Mobile: 91-7506449333; e-mail: info@crystalclearproducts.org

e-mail: info@crystalclearproducts.org

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